Optimize Analysis of Polar and Coeluting VOCs in Whole Air Canister Samples Using an Rtx®-VMS GC Column

Applications | 2016 | RestekInstrumentation
GC/MSD, Thermal desorption, Purge and Trap, GC/SQ, Consumables
Industries
Environmental
Manufacturer
Agilent Technologies, Markes, Restek
Key words
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TO-15 65 Component Mix on Rtx®-VMS (30 m)
|Agilent Technologies|Applications
TO-15 65 Component Mix on Rtx®-VMS (30 m)1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.31.32.33.34.35.PeaksPropyleneDichlorodifluoromethane (Freon® 12)1,2-Dichlorotetrafluoroethane (Freon® 114)ChloromethaneVinyl chloride1,3-ButadieneBromomethaneChloroethaneTrichlorofluoromethane (Freon® 11)1,1-DichloroetheneCarbon disulfideEthanol1,1,2-Trichlorotrifluoroethane (Freon® 113)AcroleinIsopropyl alcoholMethylene chlorideAcetonetrans-1,2-DichloroetheneHexaneMethyl tert-butyl ether (MTBE)Acetonitrile (contaminant)1,1-DichloroethaneVinyl acetatecis-1,2-DichloroetheneCyclohexaneBromochloromethane (IS)ChloroformCarbon tetrachlorideEthyl acetateTetrahydrofuran1,1,1-Trichloroethane2-Butanone (MEK)HeptaneBenzene1,2-DichloroethanetR (min)1.421.461.601.631.721.752.012.132.262.672.682.702.722.963.143.143.193.263.333.373.573.753.974.184.334.344.404.504.524.534.564.664.844.875.0436.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.66.67.68.69.70.54,55PeaksTrichloroethylene1,4-Difluorobenzene (IS)1,2-DichloropropaneBromodichloromethaneMethyl methacrylate1,4-Dioxanecis-1,3-DichloropropeneTolueneTetrachloroethene4-Methyl-2-pentanone (MIBK)trans-1,3-Dichloropropene1,1,2-TrichloroethaneDibromochloromethane1,2-Dibromoethane2-Hexanone (MBK)Chlorobenzene-d5 (IS)ChlorobenzeneEthylbenzenem-Xylenep-Xyleneo-XyleneStyreneBromoform4-Bromofluorobenzene*1,1,2,2-Tetrachloroethane4-Ethyltoluene1,3,5-Trimethylbenzene1,2,4-Trimethylbenzene1,3-Dichlorobenzene1,4-DichlorobenzeneBenzyl chloride1,2-DichlorobenzeneHexachlorobutadiene1,2,4-TrichlorobenzeneNaphthalenetR (min)5.365.405.835.896.056.116.486.707.077.107.137.297.467.707.988.258.278.318.488.488.969.029.039.659.929.9610.0810.5510.9211.0411.3711.5713.1413.1513.42*Tuning standard57,584451,525333,34366328,29,301918 201.0064 6567426049...
Key words
xylene, xylenechloride, chloridevinyl, vinylscan, scannutech, nutechcryofocuser, cryofocusermin, mindisulfide, disulfideacetate, acetatepreconcentrator, preconcentratorcarbon, carbonmethyl, methylacrolein, acroleinbfb, bfbstandard
Rapid Determination of TO-15Volatile Organic Compounds (VOCs) in AirBy Jason S. HerringtonAbstractThe following study evaluated the efficacy of using Nutech’s 8900DS preconcentrator in combination with an analytical systembased on a 30 m x 0.32 mm x 1.00 µm Rxi®-5Sil MS...
Key words
bdl, bdlpptv, pptvtimeout, timeoutppbv, ppbvaudit, audittime, timevinyl, vinylchloride, chloridemdl, mdlreplicate, replicateaverage, averageflow, flowprecision, precisiondesorb, desorbpurge
Environmental ApplicationsWhole Air Canister Sampling andPreconcentration GC-MS Analysis for pptvLevels of Trimethylsilanol in SemiconductorCleanroom AirBy Jason S. Herrington, Ph.D.AbstractThe costly damage trimethylsilanol (TMS) in cleanrooms exacts on scanner lenses in the semiconductor industry has resulted inthe demand for accurate and...
Key words
timeout, timeouttrimethylsilanol, trimethylsilanoltime, timepptv, pptvmeasurements, measurementsadl, adlreplicate, replicateblanks, blanksflow, flowstandard, standarddesorb, desorbpurge, purgeflush, flushlimit, limitcanister
Foods, Flavors & FragrancesAnalysis of Nicotine and Impurities inElectronic Cigarette Solutions and VaporBy Jason S. Herrington, Colton Myers, and Amanda RigdonAbstractElectronic cigarettes (e-cigarettes) are growing in popularity exponentially. Despite their ever-growing acceptance, relatively littlework has been done to characterize their...
Key words
orange, orangeblue, bluegreen, greenred, rednicotine, nicotinecigarette, cigarettemarkes, markesvapor, vapormin, minunity, unityscan, scangas, gasoven, ovencarrier, carriertrap