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Routine-grade performance of a new static headspace autosampler for the analysis of residual solvents according to USP <467> method

 

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Enhanced Productivity for Residual Solvent Analysis in Pharmaceutical Products According to USP 467 by Using a New Valve-and-Loop Static Headspace Sampler Xiaoteng Gong1, Benjamin Webber1, Gayatri Trivedi1, Danny Hower1, Dujuan Lu1, Julian Gulbinski1, Cristian I. Cojocariu2, Giulia Riccardino2, Daniela Cavagnino3,…
Key words
xylene, xylenedmso, dmsowater, waterresidual, residualpharmaceutical, pharmaceuticalprocedure, proceduredichloromethane, dichloromethanesoluble, solublesolvents, solventswere, weremethylcyclohexane, methylcyclohexanediluted, dilutedinsoluble, insolublerepeatability, repeatabilityinstant
Analysis of USP <467> Residual Solvents using Agilent J&W DB‑WAX Ultra Inert Capillary GC Columns Following USP <467> Residual Solvents Procedure B Application Note Pharmaceutical Authors Abstract Yun Zou and Weihua Jia This application note highlights the excellent performance of…
Key words
wax, waxxylene, xyleneresidual, residualagilent, agilentsolvents, solventsfid, fiddichloromethane, dichloromethanemethylcyclohexane, methylcyclohexaneacetonitrile, acetonitrilecyclohexane, cyclohexanemin, minpyridine, pyridinechlorobenzene, chlorobenzenetetrahydrofuran, tetrahydrofurandeactivated
TECHNICAL NOTE 10679 Routine-grade quantitative performance of TriPlus 500 Headspace Autosampler coupled to TRACE 1310 GC-FID Authors Introduction Giulia Riccardino and Cristian Cojocariu, Thermo Fisher Scientific, Runcorn, UK. Testing pharmaceutical products for their potential residual solvents that are used or…
Key words
xylene, xyleneich, ichsolvents, solventsinstant, instantresidual, residualconnect, connectfid, fidtemplates, templatesvolatile, volatilechlorobenzene, chlorobenzenetetrachloride, tetrachloriderecomendations, recomendationsthrichloroethene, thrichloroetheneethylbenzene, ethylbenzenegiulia
AppNote 9/2009 Implementation of USP <467> “Residual Solvents” using a GERSTEL MPS 2 Syringe Based Headspace Autosampler John R. Stuff, Jacqueline A. Whitecavage Gerstel, Inc., 701 Digital Dr. Suite J, Linthicum, MD 21090, USA KEYWORDS Static Headspace, Residual Solvents, USP…
Key words
zebrontm, zebrontmacetonitrile, acetonitrilegerstel, gerstelxylene, xylenebenzene, benzenetetralin, tetralinnitromethane, nitromethaneheadspace, headspacemethylcyclohexane, methylcyclohexanetrichloroethene, trichloroethenemin, mincyclohexane, cyclohexanepyridine, pyridinesuitability, suitabilitychlorobenzene
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