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TMSI + Pyridine - Product Specification
1997|Merck|Brochures and specifications
TMSI+Pyridine Product Specification TMSI (N-trimethylsilylimidazole) is the strongest reagent for hydroxyls. It reacts quickly and smoothly with hindered and unhindered hydroxyl and carboxyl groups. TMSI+Pyridine is useful for derivatizing wet sugar samples, hindered hydroxyl groups in steroids and, in conjunction…
Key words
derivatives, derivativessilyl, silylsilylating, silylatingnch, nchderivatization, derivatizationtms, tmstmsi, tmsistorage, storagereagent, reagentsilylation, silylationhandbook, handbookawr, awrreaction, reactionprocedure, procedurereactions
N-t-Butyldimethylsilylimidazole - Product Specification
1997|Merck|Brochures and specifications
N-t-Butyldimethylsilylimidazole Product Specification N-t-Butyldimethylsilylimidazole (TBDMSIM) is formed by reacting butyldimethylchlorosilane and imidazole (1:2). Although TBDMSIM is not widely used, the t-butyldimethylsilyl (TBDMS) derivatives it forms enhance thermal stability and increase the inertness of the analyte(s). A weak silylating reagent, TBDMSIM…
Key words
derivatives, derivativestbdms, tbdmssilyl, silylnch, nchbutyldimethylsilylimidazole, butyldimethylsilylimidazolestorage, storagereagent, reagentsilylating, silylatinggroup, groupstability, stabilityhandbook, handbookleaving, leavingsilicon, siliconethers, ethersbff
TMCS - Product Specification
1997|Merck|Brochures and specifications
TMCS Product Specification TMCS (trimethylchlorosilane) is a silylation catalyst, rarely used alone in analytical applications but typically mixed with other silylation reagents to increase their reactivity (e.g., HMDS/TMCS/ pyridine, BSTFA/TMCS, BSA/TMCS) in derivatization of alcohols, alkaloids, amines, biogenic amines, carboxylic…
Key words
silyl, silylderivatives, derivativesderivatization, derivatizationstorage, storagesilylating, silylatingbfe, bfereaction, reactionprocedure, proceduresilyating, silyatingtrialkylsilyl, trialkylsilylmicroreaction, microreactiontmcs, tmcsunopened, unopenednucleophilic, nucleophilicbasicity
Bulletin 909A Guide to Derivatization Reagents for GC A large number of reagents are used to prepare derivatives for gas chromatography, but most of the derivatization reactions fit into one of three categories: acylation, alkylation, or silylation. This bulletin describes…
Key words
trimethylsilyl, trimethylsilylethers, etherstmcs, tmcstmsi, tmsibstfa, bstfaalkylation, alkylationsilylation, silylationesters, estershmds, hmdsacylation, acylationdmf, dmfsupelco, supelcobsa, bsadialkylacetals, dialkylacetalsamides
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