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Consumables and accessories - For GC sample extraction

Brochures and specifications |  | MarkesInstrumentation
HeadSpace, SPME, Thermal desorption, Consumables
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Summary

Importance of the Topic


Reliable sampling of trace volatile and semi-volatile organic compounds is essential for accurate environmental monitoring, food and beverage quality control, clinical diagnostics and industrial process testing. Consumables and accessories tailored for gas chromatography (GC) not only simplify sample preparation but also improve analytical sensitivity, reproducibility and laboratory throughput.

Objectives and Study Overview


This catalogue from a leading GC-sampling specialist presents a comprehensive range of consumables and accessories designed to support headspace (HS), solid-phase microextraction (SPME), high-capacity sorptive extraction (HiSorb) and thermal desorption (TD) workflows. It also introduces Centri®, a multi-mode automated extraction and enrichment platform, demonstrating how tailored hardware can extend analytical capability to tackle challenging solid, liquid and gas samples.

Methodology and Instrumentation


Key sampling approaches include:
  • Static headspace: minimal preparation for very volatile compounds with optional cryo-free focusing traps to sharpen peaks and remove water.
  • SPME: solvent-free extraction using coated fibers for improved selectivity, with both manual and automated Centri-based trap refocusing modes.
  • HiSorb: robust probes with high-capacity sorptive phases for direct immersion or headspace sampling of complex matrices, desorbed offline or via Centri.
  • Thermal desorption: tube-based workflows using conditioned sorbent tubes for offline analysis or full automation in Centri.

Supporting accessories cover syringes, vials and caps, fiber assemblies, agitation blocks, injector liners and cryo-free focusing traps. Centri modules accommodate multiple sampling modes and include precision temperature and flow controls, enabling overlap enrichment, quantitative re-collection and automated wash sequences.

Main Findings and Discussion


Integrating a cryogen-free focusing trap significantly lowers detection limits and improves peak shapes without compromising symmetry. Comparative data show that SPME–trap workflows on Centri can detect up to 229 compounds in a tea sample versus 82 using conventional SPME. Enhanced headspace volumes and multi-stage enrichment further increase analyte coverage for odourants at sub-ppt levels.

Benefits and Practical Applications


  • Food and beverage flavour and aroma profiling
  • Environmental pollutant quantification in soil, water and air
  • Clinical biomarker analysis in blood and urine
  • Metabolite screening in biological matrices
  • Industrial QA/QC of solvents and packaging residues

Future Trends and Opportunities


Advances in cryogen-free refocusing, modular autosamplers and high-capacity probes will drive higher throughput and lower per-sample costs. Emerging areas include coupling automated multi-mode extraction with high-resolution MS, real-time screening in process environments and AI-guided method optimization. Miniaturized and portable versions of these technologies may open new applications in field sampling and point-of-care testing.

Conclusion


This suite of consumables, accessories and the Centri platform delivers a versatile, automated and high-sensitivity solution for GC sampling across diverse matrices. By optimizing each step—from extraction to injection—laboratories can achieve lower detection limits, broader compound coverage and greater efficiency.

References


No additional references provided in the source document.

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