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AC BioDiesel All in One Analyzer

Brochures and specifications | 2020 | PACInstrumentation
GC
Industries
Energy & Chemicals
Manufacturer
Agilent Technologies, PAC

Summary

Significance of Biodiesel Analysis


Biodiesel derived from fatty acid methyl esters (FAME) represents a sustainable alternative to fossil diesel, contributing to greenhouse gas reduction and compliance with global renewable fuel mandates. Reliable analysis of FAME quality is essential for environmental, regulatory, and fuel performance standards.

Study Overview


The AC Analytical Controls All-In-One Biodiesel Analyzer integrates multiple standardized gas chromatography methods into a single system to assess critical FAME parameters. Fully compliant with EN 14214 and ASTM D6751, the system evaluates ester content, glycerol species, methanol, and iodine value for blends and pure biodiesel.

Methodology and Instrumentation


This solution employs an Agilent 8890 Series gas chromatograph equipped with electronic pneumatic control and a proprietary AC TPI inlet. Key features include:
  • Dual programmable oven design hosting two capillary columns for simultaneous FAME and triglyceride analysis without manual column swaps
  • Split/splitless inlet and two flame ionization detectors for sensitive quantification
  • Dedicated software with automated method templates, QC checks, and pass/fail reporting against specifications

Main Results and Discussion


Validation demonstrates that the All-In-One Analyzer consistently meets regulatory limits: ester content ≥96.5 % m/m, linolenic acid methyl ester ≤12 % m/m, free glycerol ≤0.02 % m/m, total glycerol ≤0.25 % m/m, methanol ≤0.20 % m/m, and iodine value ≤120 g I₂/100 g. Repeatability metrics align with EN and ASTM method requirements, confirming robust performance and minimal operator intervention.

Benefits and Practical Applications


The integrated platform offers labs a streamlined workflow, high throughput, and reduced downtime. Significant advantages include:
  • True all-in-one analysis with no column changes or complex setup
  • Enhanced uptime through automated performance checks and QC samples
  • Comprehensive traceability via software-enabled calibration and audit-ready reports

Future Trends and Opportunities


Emerging developments may include expanded PUFA determination, real-time process monitoring, enhanced connectivity for remote diagnostics, and integration of advanced detectors for broader biofuel components analysis.

Conclusion


The AC All-In-One Biodiesel Analyzer provides a fully compliant, efficient, and reliable solution for biodiesel quality control. Its unique dual oven design and dedicated software streamline laboratory operations, ensuring consistent adherence to international standards.

References


  • EN 14214: Fatty Acid Methyl Esters (FAME) for Biodiesel – Requirements and Test Methods
  • ASTM D6751: Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
  • EN 14103: Determination of Ester and Linolenic Acid Methyl Ester Content
  • EN 14105: Determination of Free Glycerol and Glycerides
  • EN 14110: Determination of Methanol Content
  • ASTM D6584: Determination of Glycerin Content

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