Pressure-Balanced Headspace for the Determination of Class I, II and III Residual Solvents in Pharmaceuticals by USP Chapter <467> Methodology | LabRulez GCMS
 

Similar PDF

Toggle
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Key words
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
Capillary GC ColumnChoices for ResidualSolvent AnalysesUsing Direct Injection orSolid Phase Microextraction(SPME)The life science businessof Merck operates asMilliporeSigma in theU.S. and Canada. In the process of preparing a pharmaceutical product, you can potentially retain residualorganic solvents in the final preparation. In the...
Key words
dipole, dipolespme, spmefiber, fiberacetate, acetateresidual, residualretention, retentioncolumn, columnheadspace, headspacechoices, choicesanalytes, analytesidentification, identificationtime, timebutanol, butanolsolvents, solventsimmersion
A P P L I C AT I O N N O T EGas ChromatographyAuthor:David ScottPerkinElmer, Inc.Shelton, CTResidual Solvents inPharmaceuticals by USPChapter <467> MethodologyIntroductionThe synthesis of activepharmaceutical ingredients(API) may require multiplereaction steps that produceundesirable reaction byproducts or utilize various solvents...
Key words
headspace, headspacesolvents, solventsresidual, residualpressure, pressurevial, vialintegration, integrationwithdraw, withdrawsampler, samplerscott, scottreaction, reactionrequire, requireexperimental, experimentalpermissible, permissibleturbomatrix, turbomatrixbalanced
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Key words
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
 

Similar PDF

Toggle
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Key words
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
Capillary GC ColumnChoices for ResidualSolvent AnalysesUsing Direct Injection orSolid Phase Microextraction(SPME)The life science businessof Merck operates asMilliporeSigma in theU.S. and Canada. In the process of preparing a pharmaceutical product, you can potentially retain residualorganic solvents in the final preparation. In the...
Key words
dipole, dipolespme, spmefiber, fiberacetate, acetateresidual, residualretention, retentioncolumn, columnheadspace, headspacechoices, choicesanalytes, analytesidentification, identificationtime, timebutanol, butanolsolvents, solventsimmersion
A P P L I C AT I O N N O T EGas ChromatographyAuthor:David ScottPerkinElmer, Inc.Shelton, CTResidual Solvents inPharmaceuticals by USPChapter <467> MethodologyIntroductionThe synthesis of activepharmaceutical ingredients(API) may require multiplereaction steps that produceundesirable reaction byproducts or utilize various solvents...
Key words
headspace, headspacesolvents, solventsresidual, residualpressure, pressurevial, vialintegration, integrationwithdraw, withdrawsampler, samplerscott, scottreaction, reactionrequire, requireexperimental, experimentalpermissible, permissibleturbomatrix, turbomatrixbalanced
595 North Harrison RoadBellefonte, PA 16823-0048 USATelephone 800-247-6628 • 814-359-3441Fax 800-447-3044 • 814-359-3044email: supelco@sial.comsigma-aldrich.com/supelcoBulletin 933Capillary GC Column Choices for Residual Solvent AnalysesUsing Direct Injection or Solid Phase Microextraction* (SPME)There is a variety of solvents used in pharmaceutical processing. In the...
Key words
dipole, dipolespme, spmesupelco, supelcoacetate, acetateresidual, residualsolvents, solventsretention, retentionheadspace, headspaceidentification, identificationmin, minbutanol, butanoltime, timeimmersion, immersionxylene, xylenebutyl
 

Related content

Accurate Mass Library for Natural Products Based on Compounds Identified in Hemp Oil Using High-Resolution GC/Q-TOF

Applications
| 2022 | Agilent Technologies
Instrumentation
GC/MSD, GC/MS/MS, GC/HRMS, GC/Q-TOF
Manufacturer
Agilent Technologies
Industries
Food & Agriculture

Analysis of Polycyclic Aromatic Hydrocarbons (PAH) in Palm Oil by GC-MS/MS

Applications
| 2022 | Shimadzu
Instrumentation
GC/MSD, GC/MS/MS, GC/QQQ
Manufacturer
Shimadzu
Industries
Food & Agriculture

Determination of Polycyclic aromatic hydrocarbons in soils using the EXTREVA ASE Accelerated Solvent Extractor and GC-MS

Applications
| 2022 | Thermo Fischer Scientific
Instrumentation
GC/MSD, Sample Preparation, GC/SQ
Manufacturer
Thermo Fischer Scientific
Industries
Environmental

Comprehensive Evaluation of Scotch Whisky Aroma Profiles Using SPME-GCxGC-TOFMS

Applications
| 2022 | LECO
Instrumentation
GCxGC, GC/MSD, SPME, GC/TOF
Manufacturer
LECO
Industries
Food & Agriculture

NEMC: Increasing Sample Throughput in Ultra-trade Environmental Analysis with the TSQ-9610 GC- MS/MS

Presentations
| 2022 | Thermo Fischer Scientific
Instrumentation
GC/MSD, GC/MS/MS, GC/QQQ
Manufacturer
Thermo Fischer Scientific
Industries
Environmental
 

Related content

Accurate Mass Library for Natural Products Based on Compounds Identified in Hemp Oil Using High-Resolution GC/Q-TOF

Applications
| 2022 | Agilent Technologies
Instrumentation
GC/MSD, GC/MS/MS, GC/HRMS, GC/Q-TOF
Manufacturer
Agilent Technologies
Industries
Food & Agriculture

Analysis of Polycyclic Aromatic Hydrocarbons (PAH) in Palm Oil by GC-MS/MS

Applications
| 2022 | Shimadzu
Instrumentation
GC/MSD, GC/MS/MS, GC/QQQ
Manufacturer
Shimadzu
Industries
Food & Agriculture

Determination of Polycyclic aromatic hydrocarbons in soils using the EXTREVA ASE Accelerated Solvent Extractor and GC-MS

Applications
| 2022 | Thermo Fischer Scientific
Instrumentation
GC/MSD, Sample Preparation, GC/SQ
Manufacturer
Thermo Fischer Scientific
Industries
Environmental

Comprehensive Evaluation of Scotch Whisky Aroma Profiles Using SPME-GCxGC-TOFMS

Applications
| 2022 | LECO
Instrumentation
GCxGC, GC/MSD, SPME, GC/TOF
Manufacturer
LECO
Industries
Food & Agriculture

NEMC: Increasing Sample Throughput in Ultra-trade Environmental Analysis with the TSQ-9610 GC- MS/MS

Presentations
| 2022 | Thermo Fischer Scientific
Instrumentation
GC/MSD, GC/MS/MS, GC/QQQ
Manufacturer
Thermo Fischer Scientific
Industries
Environmental
Other projects
Follow us
More information
WebinarsAbout usContact usTerms of use

LabRulez s.r.o., all rights reserved.